Alcohols, Phenols and Ethers: Speed-Solving Techniques (4)

easy 2 min read

Question

Predict the major product when 2-methylbutan-2-ol is treated with concentrated H2SO4H_2SO_4 at 170°C170°C. Explain the mechanism in two lines. Also predict whether Saytzeff or Hofmann’s rule applies. NEET 2023 pattern.

Solution — Step by Step

2-methylbutan-2-ol is (CH3)2C(OH)CH2CH3(CH_3)_2C(OH)CH_2CH_3. Concentrated H2SO4H_2SO_4 at high temperature performs acid-catalysed dehydration — an E1 elimination producing an alkene.

Protonation of OH-OH gives a leaving group (water). Loss of water generates a tertiary carbocation: (CH3)2C+CH2CH3(CH_3)_2C^+CH_2CH_3. Tertiary carbocations are stable, so no rearrangement occurs.

Saytzeff (Zaitsev) says: the more substituted alkene is the major product. We have two β-positions: a CH3-CH_3 (with 3 H’s) and a CH2CH3-CH_2CH_3 (with 2 H’s, leading to a more substituted double bond).

Eliminating from CH2CH3-CH_2CH_3 gives 2-methyl-2-butene (trisubstituted). Eliminating from CH3-CH_3 gives 2-methyl-1-butene (disubstituted).

Major product: 2-methyl-2-butene (CH3)2C=CHCH3(CH_3)_2C=CHCH_3 (trisubstituted alkene, Saytzeff product). Hofmann’s rule does not apply here — that’s for elimination with bulky bases (E2 with tBuOtBuO^-), not acid-catalysed E1.

Why This Works

E1 dehydration always favours the most stable alkene because the rate-determining step is carbocation formation, but the product distribution is controlled by the relative stability of the alkenes — and more substituted alkenes are more stable (hyperconjugation, ground-state effect).

This is exactly Saytzeff’s rule: most substituted alkene wins. Hofmann’s rule (least substituted) only applies in special cases like quaternary ammonium thermolysis or E2 with bulky bases that can’t reach the more hindered β-hydrogen.

Alternative Method

Use the carbocation stability check. For tertiary alcohols + acid, you always get E1 with no rearrangement. Just identify the most stable alkene from the two β-elimination options. No need to write the full mechanism for a 1-mark MCQ.

Students often pick Hofmann’s product (less substituted) for acid-catalysed dehydration. Wrong context: Saytzeff applies to E1 and standard E2 with small bases. Hofmann applies to E2 with bulky bases or thermolysis of quaternary ammonium hydroxides.

Memorise: alcohol + conc. acid + heat = E1 = Saytzeff. Alkyl halide + bulky base (KOtBu) = E2 with Hofmann tendency. Know the conditions that flip the rule.

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